ヒト血清中の内因性ステロイド物質(13種)の同時定量分析

	Compound	Ion Mode	RT ( min )	MRM	LOQ ( ng/mL )	Range ( ng/mL )	Blank Serum ( ng/mL )
1	DHEAS	ESI -	1.05	367.2 > 97.0	0.0025	0.0025 - 25	1360
2	Estriol	ESI -	2.00	237.2 > 17.10, 145.0	0.05	0.05 - 250	n.d.
3	Aldosterone	ESI +	2.32	361.3 > 343.3, 315.2	0.005	0.005 - 50	n.d.
4	Cortisol	ESI +	3.21	363.2 > 327.2, 121.1	0.0025	0.0025 - 25	149
5	Corticosterone	ESI +	4.41	347.3 > 329.3, 311.2	0.01	0.01 - 25	2.94
6	11-Deoxycortisol	ESI +	4.78	347.3 > 109.1, 97.0	0.0025	0.0025 - 25	0.22
7	Androsteronedione	ESI +	5.65	287.2 > 109.1, 97.0	0.0025	0.0025 - 25	0.77
IS	Estradiol-d5	ESI -	5.70	276.2 > 147.1
8	Estradiol	ESI -	5.72	271.2 > 183.1, 145.1	0.05	0.05 - 500
9	Estrone	ESI -	5.82	269.2 > 183.1, 145.1	0.05	0.05 - 500	u'q'
IS	Testosterone-d3	ESI +	6.24	292.2 > 97.0			u'q'
10	Testosterone	ESI +	6.27	289.2 > 97.0	0.0025	0.0025 - 25
11	17α - Hydroxyprogetserone	ESI +	6.68	331.3 > 109.1, 97.0	0.0025	0.0025 - 25	3.94
IS	DHEA-d5	ESI +	6.93	276.2 > 258.2			0.24
12	DHEA	ESI +	6.96	271.2 > 253.2, 197.2	0.025	0.0025 - 250	n.d.
IS	Progesterone-d9	ESI +	8.30	324.3 > 100.2
13	Progesterone	ESI +	8.30	315.3 > 109.2, 97.0	0.0025	0.0025 - 25	0.05

Counts vs. Acquisition Time (min)